ICPMS-2030 LF Inductively Coupled Plasma Mass Spectrometer

The ICPMS-2030 LF is quantitative and qualitative mass analyzer having an inductively coupled plasma ion source. This instrument is a very convenient for element analysis of solution sample and superior to ICP emission spectrometers, in detecting sensitivity.

Description

HIGHLIGHTS

With its newly developed collision cell and optimized internal structure, the ICPMS-2030 provides superior sensitivity. At the same time, thanks to the adoption of its proprietary mini-torch unit and provision of an Eco mode, the quantity of argon gas needed for analyses has been greatly reduced to the industry’s lowest levels. As a result, low running costs are assured. The Development Assistant function of the software automatically sets the optimal analysis conditions for quantitative analysis. Then, after measurements are complete, the Diagnosis Assistant function automatically checks the validity of the necessary data. While reducing the burden on the user, the efficiency of analyses is enhanced and the reliability of the data can be increased. It complies with FDA 21 CFR Part 11

Accelerating Reliable Performance
The first system in the industry to include functions for assisting with analytical method development and diagnostics.
Newly developed collision cell and On-Line IEC work together to eliminate spectral interference, and achieve high-sensitive and low-interference analyses.
Unique system developed by Shimadzu results in the industry’s lowest running costs.

Plasma Ion Source Unit
Spray chamberCyclone chamber

(Thermoelectric cooling type: -10 °C to 10 °C)

Peristaltic pump4-channel, 12 roller pump
Plasma torchQuarts-made mini torch
NebulizerHigh Efficiency Concentric (coaxial) nebulizer

Made of borosilicate glass

Torch position adjustmentX,Y,Z-axes automatic adjustment

Horizontal and vertical position range:

±2 mm (0.1 mm step)

Sampling depth:2 to 12 mm

Plasma ViewEasy-View window for visual monitoring of plasma to check torch, RF coil
Gas controlGas flowrate is auto controlled from CPU

Flowrate setting range

Plasma gas (Ar) 7 to 20 L/min

Auxiliary gas (Ar) 0.3 to 1.5 L/min

Carrier gas (Ar) 0.3 to 1.5 L/min

Economy running mode (Mini-Torch)Plasma gas (Ar) 5 L/min

Auxiliary gas (Ar) 0.6 L/min

RF Power Supply Unit
TransmitterFree running
Frequency27 MHz
RF Power0.5 kW (Eco mode) and 0.8 kW to 1.4 kW (1.2 kW when using mini torch)
Output stabilityWithin ±0.3 %
Radio-frequency circuit elementAll solid state
Ignition methodFull automatic ignition
Load matching functionAutomatic matching
Energy saving functionEconomic running mode
Interface
Sampling coneCu sampling cone 1.1 mm diameter orifice (Option: Ni, Pt)
Skimmer coneCu skimmer cone 0.35 mm diameter orifice (Option: Ni, Pt)
Removable interface to deviceNo tool required

Interface system designed with easy access for maintenance

Ion LensAdvanced Off-axis lens after Cell
Delivers high ion transfer efficiency
Collision cell
TypeOctopole collision cell
Gas controllerGas flowrate is auto controlled from CPU (Used gas: Helium gas)

– Flowrate setting range: 0 to 10 mL/min

Mass Spectrometer Unit
Mass analyzerQuadruple type mass spectrometer

Molybdenum-made hyperbolic rod (Main rod)

Molybdenum-made cylindrical rod (Pre-rod)

Power supply frequency2.5 MHz
Mass range5 to 260 amu
Resolution0.5 u to 1.0 u (at 5 to 225 amu) *
Mass Accuracy±0.1 u (209Bi)
Mass Stability0.03 u / 24 Hr (115In)
Abundance sensitivity (at 133Cs)Low mass side ≦5×10-7

High mass side ≦1×10-7

Detector
DetectorDual-mode electron multiplier
Dynamic range9 order (1 cps to 109 cps)
Minimum dwell time1 msec
Exhaust system3-stage operation exhaust
First stage Rotary pump
2nd stage, 3rd stage Air-cooling type turbo molecular pump
Performance Specifications
Sensitivity (Mcps/ppm)
9Be> 6
115In>125
209Bi>100
Detection Limit (ppt)
9Be<0.5
115ln<0.1
209Bi<0.1
Background (CPS)
m/Z 220<1
Oxide ratio (%)
CeO/Ce<2
Doubly Charge(%)
Ce++/Ce<3
Stability %RSD
Short Term< 3% (20 min)
Long Term< 4% (4 Hr)
He Cell Mode
Co (Mcps/ppm)> 6
DimensionsW 870 x D 645 x H 587 mm (excluding protrusion)
Weight
Main body140 kg
Rotary Pump50 kg
Temperature18 °C to 28 °C (max. 2 °C/h temperature change)
Humidity20 to 70% RH (No condensation)
OtherAvoid using the system in locations with significant vibration or dust
Power Supply
Main UnitSingle-phase 200 to 240 V ± 10 %, 50/60 Hz, 6 kVA
Data ProcessingSingle-phase 100 to 240V ± 10 %, 50/60 Hz, 200 VA
Cooling Water Circulator (Option)Single-phase 200 to 230 V, 50/60 Hz, 2 kVA
GroundingUse the single earth of the ground resistance 30 Ω max
Gas Supply
Argon gas99.95 % or more purity, Pressure 450±10 kPa
Helium gas99.999 % or more purity, Pressure 150±20 kPa
Cooling Water
Pressure150 to 300 kPa
Temperature5 to 30 °C
Exhaust DuctAdjusting to the displacement of 1.4 to 2 m3/min is possible at the outlet of the main body exhaust cylinder
Environmental, Drinking Water, and Wastewater Analysis
Food Products/Agriculture
Pharmaceuticals/Pharmacopoeia
AS-10 Autosampler
Vials:60 15-mL vials
8 50-mL vials
SizeW290 × D508 × H300 mm (excluding arm)
Power supplySingle-phase 100–240 V, 50/60 Hz, 50 VA
ASX-560 Autosampler
Vials:10 50-mL vials (standard samples) or
240 14-mL vials
160 20-mL vials (rack sold separately)
84 50-mL vials (rack sold separately)
SizeW580 × D550 × H620 mm
(include sample probe)
W90 × D180 × H60 mm
(rough dimensions of power supply unit)
Power supply100-240 V AC, 47-63 Hz, 1.9 A
ASX-280 Autosampler
Vials:10 50-mL vials (standard samples) or
120 14-mL vials
80 20-mL vials (rack sold separately)
42 50-mL vials (rack sold separately)
SizeW355 × D550 × H620 mm
(include sample probe)
W90 × D180 × H60 mm
(rough dimensions of power supply unit)
Power supply100-240 V AC, 47-63 Hz, 1.9A
Cooling Water Circulator
SizeW377 × D500 × H615 mm
Power supplyAC 200 V–230 V, 50/60 Hz, 2 kVA
Weight43 kg
Automatic Internal Standard Addition KitThis kit is used for in-line mixing of measurement sample and internal standard solutions and introducing the mixtures into the ICP system.
Tap Water Connection KitThis is required if using tap water to cool the main ICPMS-2030 unit.
Noise Absorbing Box, SV65 Large
Exhaust Duct Connection AdapterNeeded when connecting a flexible duct made of stainless steel having an internal diameter of 100 mm to the exhaust duct of the plasma stand.
HFS-5 Hydrofluoric Acid Sample Injection SystemThis system includes a torch, chamber, extension tube, nebulizer, drain, and their corresponding accessory parts.
Used to directly inject samples that contain hydrofluoric acid. The nebulizer, chamber, and drain system are made using fluoropolymer materials and the injector unit on the torch is made using alumina.
Organic Solvent Injection SystemTo introduce organic solvents, a mixture of argon and oxygen gases (70% Ar and 30% O2 ) is injected into the interface unit to prevent precipitation of carbon (C) by the organic solvent. This system includes a Quadruple Torch for Organic Solvents, ICPMS, drain, and their corresponding accessory parts.
LC–ICP–MS SystemIt can be used as the LC–ICP–MS system by connecting the ICPMS-2030 and the Prominence™ inert LC system online
LA–ICP–MS System (Laser Ablation ICP–MS System)The LA–ICP–MS system can be set by combining the ICPMS-2030 and other companies’ laser ablation equipment.
Measurement sample
1 data fileMaximum 300 samples
Pasting of sample informationIt is possible to paste the sample information to the sample table from the clip board
Qualitative analysis
Method of analysisAnalysis using the built-in data base
Selecting Mass numberSelect the optimum mass in auto every measurement sample
CorrectionThe data base calibration function is available
Quantitative analysis
Measured massIt is possible to set the multiple measured mass every elements.

Total mass profile measurement

Correction methodInternal standard correction, inter-element correction, interference correction, drift correction, dilute correction
Calibration curveFirst to secondary equation

Quantitative lower limit display

PrintingSetting for the printing items

Automatic printing when measuring (Analysis results)

Batch printing (Analysis conditions/ calibration curves/ analysis results, etc.)

Copy of the display windowUse a clip board function of the Windows, and copying is possible to other applications such a
Export of the dataIt is possible to output the analyzed results to the files in a CSV format or a tab delimited text format.

Automatic export when measuring

Batch export

Re-calculation functionChanges of the calibration curve conditions such as the calibration curve order

Re-calculation by changing the corrective conditions.

Add and re-calculate the analysis element/mass using the total mass profile.

Assistant function
Development assistantBased on the qualitative analysis data (for all mass numbers) from a representative sample, the Development Assistant automatically selects the optimal mass numbers and internal standard elements for the target measurement elements and automatically specifies the concentration range for calibration curve samples.
Diagnosis assistantThe Diagnosis Assistant automatically diagnoses spectral interference, based on data measured from all mass numbers.

Even when using an already established method for routine analysis, the software analyzes data for any spectral interference to determine if a problem occurred.

Instrument control
QA/QC functionsAssessment of a calibration curve and re-calibration

Fluctuation evaluation of the internal standard elements

Assessment of a drift during measuring and re-calibration / re -measurement

Addition/collection tests Dilution test

Re-measurement test

Instrument controlMonitor display for instrument status

Control vacuum pump

Plasma on/off

Automatic plasma off after analysis

Auto sampler (option) control

Economy running mode

Additional information

Manufacturer

Shimadzu

Origin

Japan

Type

Automatic

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